A simplified thin-layer chromatographic determination of hippuric acid and methylhippuric acids.

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Quantitative determination of hippuric and m-methylhippuric acids in urine by high-speed liquid chromatography.

High-speed liquid chromatography employing an ultraviolet photometric detector has been applied to the simultaneous determination of hippuric and m-methylhippuric acids in urine. Reversed-phase partition chromatography is carried out on a muBondapak C18 column with methanol-water as the eluent system. This method obviates the necessity for isolation or reaction of these acids before assay. The ...

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Thin-layer chromatography of hippuric and m-methylhippuric acid in urine after mixed exposure to toluene and xylene.

The separation of hippuric and m-methylhippuric acid as toluene and m-xylene metabolites present in urine of people exposed simultaneously to toluene and xylene is described. Chloroform was used for hippuric and m-methylhippuric acid extraction. Satisfactory separation of these metabolites was obtained on TLC plates covered with silica gels and developed in chloroform acetic acid-water (4:1:1);...

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A high-performance thin-layer chromatographic method for chlorogenic acid and hyperoside determination from berry extracts

The present study investigates a quantitative high performance thin layer chromatographic (HPTLC) method for chlorogenic acid and hyperoside determination from berry extracts. Chlorogenic acid and hyperoside were extracted using a methanol and water mixture and separated on a HPTLC 60F254 silica gel plates with ethyl acetate, acetic acid, formic acid and water 10:1.1:1.1:2.3 (v/v/v/v) as mobile...

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Measurement of urinary hippuric and m-methylhippuric acids by gas chromatography.

Buchet, J. P., and Lauwerys, R. R. (1973). British Journal ofIndustrial Medicine, 30, 125-128. Measurement of urinary hippuric and m-methylhippuric acids by gas chromatography. A gas chromatographic method for the determination of hippuric and m-methylhippuric acids in urine is described. A known amount of heptadecanoic acid (internal standard) is added to the urine before its extraction with e...

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ژورنال

عنوان ژورنال: INDUSTRIAL HEALTH

سال: 1981

ISSN: 0019-8366,1880-8026

DOI: 10.2486/indhealth.19.155